Electroless Nickel (EN) – Sodium Hypophosphite (SHP) acts as a reducing agent to supply the electrons necessary for the EN process.The EN process allows for uniform plating thickness on not only metal objects, but also plastics and ceramics. The last element is important because, while there are few manufacturers of the chemical, there are users who may come under the proposed regulations because they distribute the chemical to waste treatment facilities. Drug Traffic Control, Reporting and Recordkeeping Requirements. RESOURCES > Federal Register Notices > Rules - 2000 > Control of Red Phosphorus, White Phosphorus and Hypophosphorous Acid (and Its Salts) as List I Chemicals, [Federal Register: September 25, 2000 (Volume 65, Number 186)] Very small volumes are used to produce ultra-high-purity phosphorus semiconductor grades) for application in the electronics industry. The FCC grade meets the requirements of the Food Chemical Codex indicates and is suitable for all food, beverage and nutritional supplement applications. H 2 O. The two most common salts of hypophosphorous acid are sodium hypophosphite and manganese hypophosphite. 601. Sodium hypophosphite is a colorless hygroscopic solid, soluble in water. phosphinolate, 1-oxo-, sodium salt, hydrate (1:1:1) EC Number: 600-090-7 CAS Number: 10039-56-2 Molecular formula: NaH4PO3 IUPAC Name: phosphinolate, 1-oxo-, sodium salt, hydrate (1:1:1) Salts of hypophosphorous acid are known as hypophosphite salts. It also has applications as a reducing agent and as an antioxidant. This waste material would likely be considered a chemical mixture containing phosphorus. These phosphorus chemicals have been identified as being important chemicals for the illicit production of methamphetamine. The primary material derived from phosphate rock is white phosphorus. From the Federal Register Online via GPO Access [wais.access.gpo.gov] SUMMARY: The Comprehensive Drug Abuse Prevention and Control Act (hereinafter the "Controlled Substances Act" or "CSA") provides the Attorney General with the authority to specify by regulation, additional chemicals as "List I" chemicals if they are used in the manufacture of a controlled substance in violation of the CSA and are important to the manufacture of the controlled substance. Sodium hypophosphite explodes when titrated with chlorates or other oxidizing agents. Handlers which acquire phosphorus and convert it to non-regulated forms will not be subject to CSA regulatory requirements. It is also used as a reducing agent, analytical reagent, polymerization catalyst, polymer stabilizer, and fire retardant. The analysis identified two main producers of the hypophosphites. Quality: SMC Spec. Given our expertise spanning more than 55 years, it is the best quality product of its kind on the market. The trend continues into calendar year 2000. Red phosphorus is usually prepared as a powder and is more stable and less toxic than the white form. While chemical mixtures are currently exempt from CSA chemical regulatory requirements, the DEA is preparing regulations pertaining to such mixtures. [FR Doc. Tools The Controlled Substances Act (CSA) and its implementing regulations, specifically 21 U.S.C. Since no industry input was received in response to the Advance Notice of Proposed Rulemaking, DEA directly contacted domestic producers of elemental phosphorus and importers of phosphorus chemicals. Pricing & More Info SODIUM HYPOPHOSPHITE-1-HYDRATE, R. G., RE AGPH. The most abundant variety produced is white phosphorus (also known as yellow phosphorus). The DEA is also proposing that these salts be included as List I chemicals. No. Black phosphorus and phosphate rock will not be affected by this proposed action. Title 21 Code of Federal RegulationsTitle 21 USC Codified CSA, U.S. DEPARTMENT OF JUSTICE  •  DRUG ENFORCEMENT ADMINISTRATION Sodium hypophosphite Names IUPAC name. It is a solid at room temperature, appearing as odorless white crystals. In 1999, the DEA documented an additional 48 laboratories utilizing hypophosphorous acid. [1] With this method, a durable nickel-phosphorus film can coat objects with irregular surfaces, such as in avionics, aviation and the petroleum field. While the manganese salt is used primarily in nylon fiber production, it also has application as a chemical intermediate. Their information indicates that in southeastern Idaho, white phosphorus is frequently encountered in methamphetamine laboratories. If not confined within the reaction vessel, ingestion of this poisonous gas can result in death. Of the three chemicals subject to this proposed rule, only phosphorus is regulated under programs that require reporting to EPA. Sodium hypophosphite decomposes into phosphine which is highly irritating to the respiratory tract and disodium phosphate. Get Contact details & address of companies manufacturing and supplying Sodium Hypophosphite across India. Sodium hypophosphite has been indicated to react explosively when triturated with chlorates. Sodium Hypophosphite (DEA List I Chemical), FCC is used as an emulsifier and stabilizer. Prior to preparing this proposal the DEA also solicited information directly from importers. (ii) Red phosphorus U.S. exports totaled approximately 180 shipments of 4,300 metric tons by 32 firms. The United StatesDrug Enforcement Administration (DEA) maintains lists regarding the classification of illicit drugs (see DEA Schedules). During 1998, the DEA identified a total of only six methamphetamine laboratories utilizing hypophosphorous acid. H 2 O. If not stored in a solution, white phosphorus spontaneously combusts. EUR. This notice solicits input regarding: (1) The nature of the legitimate phosphorus industry; (2) the legitimate uses of phosphorus at all levels of distribution (including industrial uses and use by individual end-users at the retail level of distribution); (3) the potential impact such regulatory controls may have on legitimate industry (particularly with respect to the impact on small businesses); (4) the potential number of individuals/firms which may be affected by increased regulatory requirements; and (5) any other information on the manner of manufacturing, distribution, consumption, storage, disposal, and uses of phosphorus by industry and others. Hypophosphorous acid is also used as a chemical intermediate in organic syntheses and as a polymerization and polycondensation catalyst. Section 1310.04 is proposed to be amended by adding new paragraphs (g)(1)(ii) to (g)(1)(iv) to read as follows: *         *           *           *           * While producers of white phosphorus will be required to register with DEA and maintain records of each regulated transaction (i.e. What Steps Has the DEA Taken To Solicit Information From the Legitimate Phosphorus Industry? The DEA did receive six comments from law enforcement entities and two comments from Federal prosecutors in support of the control of red phosphorus as a listed chemical. Resources Companies creating MSDSs for chemicals are likely to manufacture or distribute the chemicals. It is soluble in water, and easily absorbs moisture from the air. (DEA List I Chemical) 30410 | 10039-56-2. Section 1310.02 is proposed to be amended by adding a new paragraph (a)(25) through (27) to read as follows: *         *           *          *           *, (a) * * * Since red phosphorus was the phosphorus chemical most frequently encountered in clandestine methamphetamine laboratories, the DEA initially published an Advance Notice of Proposed Rulemaking on February 2, 2000 (65 FR 4913) to solicit input from potentially affected parties regarding: (1) The nature of the legitimate red phosphorus industry; (2) the legitimate uses of red phosphorus at all levels of distribution (including industrial uses and use by individual end-users at the retail level of distribution); (3) the potential burden such regulatory controls may have on legitimate industry (particularly with respect to the impact on small businesses); (4) the potential number of individuals/firms which may be adversely affected by increased regulatory requirements; and (5) any other information on the manner of manufacturing, distribution, consumption, storage, disposal, and uses of red phosphorus by industry and others. With this method, a durable nickel-phosphorus film can coat objects with irregular surfaces, and can widely be used ionics, aviation and the petroleum field. Sodium phosphinate. It is a solid at room temperature, appearing as odorless white crystals. Global Sodium Hypophosphite Market. What Portion of the Phosphorus Industry Is Potentially Impacted by This Regulation? sodium hypophosphite. The formula for this acid is generally written H 3 PO 2, but a more descriptive presentation is HOP(O)H 2, which highlights its monoprotic character. (1) * * * Contact most popular products of manufacturers, trading companies, wholesalers & exporter directly on Made-in-China.com 822 and 823 and 21 CFR part 1309. Sodium Hypophosphite Hydrate (DEA List I Chemical), also known as sodium phosphinate, is used for electroless nickel plating. Sodium hypophosphite, marketed under the brand name Sofibex, is manufactured in Switzerland. Controlled Substance Schedules The Drug Enforcement Administration (DEA) has determined that these controls are necessary to prevent the diversion of these chemicals to clandestine drug laboratories. New Sodium Hypophosphite products manufacturing in China, with stylish and cool design emerge. It is a critical ingredient of electroless nickel plating solutions. Medical Missions As such, recordkeeping, reporting and import/export notification requirements (as described in 21 U.S.C. DATES: Written comments must be submitted on or before November 24, 2000. Sodium Hypophosphite is used in formulating many pharmaceutical products. It is soluble in water, alcohol, and glycerol. Year-End Reports, Cases Against Doctors You are now leaving a Department of Justice Web site. SODIUM HYPOPHOSPHITE … Hypophosphorous acid shipments should be documented, but shipments of the hypophosphites may not be. Therefore, the manufacture of methamphetamine requires only small quantities of these chemicals. Sodium Hypophosphate; sodium hyposulfate; Look at other dictionaries: Hypophosphorous acid is commonly used by large industry as a bleaching, color stabilization or decoloring agent for plastics, synthetic fibers (primarily polyester) and chemicals. Chemical Intermediate – Used as a raw material in the production of other products, including Hypophosphorous Acid. Twenty-one of the 53 facilities reporting phosphorus under TRI sent phosphorus offsite to 30 separate places for treatment as waste. This notice proposes the addition of red phosphorus, white phosphorus (also known as yellow phosphorus) and hypophosphorous acid (and its salts) as List I chemicals. Based on analysis of chemistry and actual illicit use, DEA finds that these three chemicals are important to the manufacture of methamphetamine and therefore meet the definition of List I chemicals. REGULATIONS.GOV, DOJ Legal Policies and Disclaimers    |    DOJ Privacy Policy    |    FOIA    |    Section 508 Accessibility. Quota Applications Notice of Registration, Program Description 2013. 830 and 971. and 21 CFR parts 1310 and 1313) shall apply. The United States Drug Enforcement Administration (DEA) maintains lists regarding not only the classification of illicit drugs (see DEA Schedules). DEA obtained 1998 and 1999 sales data from both producers. It is a solid at room temperature, appearing as odorless white crystals. Ecological Information Environmental Fate: No information found. Why Does the DEA Believe That Control of Red Phosphorus, White Phosphorus, and Hypophosphorous Acid (and Its Salts) Is Necessary? Both quantitative and qualitative data were invited. Additionally, this notice proposes that no threshold be established for domestic and international transactions. All transactions in those substances are subject to the reporting requirements. Sodium Hypophosphite (7681-53-0) No No None 12. It is a solid at room temperature, appearing as odorless white crystals. DEA has identified only two domestic producers of white phosphorus. What Regulatory Controls Will Apply to These Chemicals? The FCC grade meets the requirements of the Food Chemical Codex indicates and is suitable for all food, beverage and nutritional supplement applications. The EN process allows for uniform plating thickness on not only metal objects, but also plastics and ceramics. The FCC grade meets the requirements of the Food Chemical Codex indicates and is suitable for all food, beverage and nutritional supplement applications. Sodium Hypophosphite (DEA List I Chemical), FCC is used as an emulsifier and stabilizer. The MSDSs located for the hypophosphites indicate. What Specific Chemicals Does This Proposed Regulation Include? [Page 57577-57581] The hypophosphites are similarly produced by very few facilities. 12. (iii) White phosphorus (Other names: Yellow Phosphorus), (iv) Hypophosphorous acid and its salts HOME        CONTACT US        A-Z SUBJECT INDEX        PRIVACY NOTICE        WEBSITE ASSISTANCE, Applications Manufacturers, distributors, importers and exporters of white phosphorus, red phosphorus and hypophosphorous acid (and its salts) will be required to register with the DEA pursuant to 21 U.S.C. According to 1999 maritime data (as reported by the Pier Import Export Reporting Service), imports of phosphorus chemicals into the U.S. totaled 101 shipments for a total of 2,500 metric tons to 36 different firms. Significant Guidance Documents DEA believes that the use of white phosphorus is under-reported. 3. H2O. From 1997 through the first quarter of 2000, 86 methamphetamine laboratories were seized in this region of Idaho. If red phosphorus alone is controlled, DEA has concluded that clandestine laboratory operators would rapidly move to white phosphorus and hypophosphorous acid. As noted above, these chemicals are used as catalysts in the illicit synthesis of methamphetamine. CMEA (Combat Meth Epidemic Act) It will not have a significant economic impact on a substantial number of small business entities. 4.2 Most important symptoms and effects, both acute and delayed To the best of our knowledge, the chemical, physical, and toxicological properties … Ungraded products supplied by Sigma Aldrich are. Additionally, hypophosphorous acid is covered in interstate commerce. 13. This regulation meets the applicable standards set forth in Sections 3(a) and 3(b)(2) of Executive Order 12988, Civil Justice Reform. Therefore, no actions were deemed necessary under the provisions of the Unfunded Mandates Reform Act of 1995. Non-California customers must complete form QAF482. DEA Forms & Applications Why Does DEA Believe That This Regulation Will Not Impose a Significant Burden on a Substantially Large Number of Firms? Identifiers CAS Number. Sodium Hypophosphite 次磷酸钠. Recently the DEA has noted a small but increasing use of hypophosphorous acid at seized clandestine laboratories. Ion Exchange Resin – It will provide a source of electrons in resin regeneration. Sodium hypophosphite, marketed under the brand name Sofibex, is manufactured in Switzerland. This data indicated that most all the material appeared to be for large industrial uses. The Deputy Administrator further certifies that this rulemaking has been drafted in accordance with the principles in Executive Order 12866 section 1(b). (37) Iodine or tincture of iodine. The EN process allows for uniform plating thickness on not only metal objects, but also plastics and ceramics. The second crystalline form is red phosphorus. Environmental Toxicity: No information found. A few reported releasing the substance to publicly owned treatment works (i.e., wastewater treatment). These analytical laboratories have historically identified seized material simply as 'phosphorus'. The Department of Justice does not endorse the organizations or views represented by this site and takes no responsibility for, and exercises no control over, the accuracy, accessibility, copyright or trademark compliance or legality of the material contained on this site. What Related Chemicals Will Not Be Subject to This Control Action? DEA TOX Toxicology Testing Program Mailing Addresses Given our expertise spanning more than 55 years, it is the best quality product of its kind on the market. SDS; Sodium hypophosphite monohydrate. Over a two-year period, the two firms had only a few customers. Hypophosphorous acid (HPA), or phosphinic acid, is a phosphorus oxyacid and a powerful reducing agent with molecular formula H 3 PO 2.It is a colorless low-melting compound, which is soluble in water, dioxane, and alcohols. Chemicals: Sodium Hypophosphite Liquid Palm's SHP is blended exclusively from high purity SHP for use in electroless nickel solutions. White phosphorus was encountered at 35 of these laboratories; red phosphorus was encountered at 27 laboratories and the type of phosphorus was not identified at 24 of these laboratories. An official version of this publication may be obtained directly from the Government Publishing Office (GPO). Sodium Hypophosphite (DEA List I Chemical), Crystal, Reagent This item is a DEA LIST 1 CHEMICAL + CALIFORNIA DOJ PRECURSOR. DEA has not been able to identify any household uses for red phosphorus, white phosphorus or hypophosphorous acid and its salts. CMEA Required Training & Self-Certification COVID-19 Information 802(39)) defines the term "regulated transaction" as a "distribution, receipt, sale, importation, or exportation of, or an international transaction involving the shipment of, a listed chemical, or if the Attorney General establishes a threshold amount for a specific listed chemical," a transaction involving a threshold amount". Sodium Hypophosphite Monohydrate 10039-56-2 231-669-9 7640mg / kg Oral - rat Not established SECTION 12: ECOLOGICAL INFORMATION 12.1 No data are available on the adverse effects of this material on the environment. Two commenters informed DEA that sodium hypophosphite, a regulated salt of hypophosphorous acid, is used in low concentrations as a stabilizer or as a catalyst. The DEA has also noted that detailed recipes describing the production of methamphetamine (using red phosphorus, white phosphorus and hypophosphorous acid) are being disseminated on the Internet. QAF482 Designation of Authorized Purchaser: DEA List 1 & 2 Chemicals QAF481 … However, these materials are being distributed in small quantities via Internet online auctions and through chemical supply houses directly to consumers. 65 Components: This product does not contain any chemicals known to State of California to cause cancer, birth defects, or any other reproductive harm Section 16. It is believed that there are few firms handling these regulated forms (i.e. Sodium hypophosphite is mainly used for electroless nickel plating (Ni-P). This rule will not result in an annual effect on the economy of $100,000,000 or more; a major increase in costs or prices; or significant adverse effects on competition, employment, investment, productivity, innovation, or on the ability of United States-based companies to compete with foreign-based companies in domestic and export markets. (28) Hypophosphorous acid and its salts (Including ammonium hypophosphite, calcium hypophosphite, iron hypophosphite, potassium hypophosphite, manganese hypophosphite, magnesium hypophosphite and sodium hypophosphite) 6797 (29) N-phenethyl-4-piperidone (NPP) 8332 (30) Iodine: 6699 (31) Ergocristine and its salts: 8612 The authority citation for part 1310 continues to read as follows: 2. Chemical Import/Export Declarations This would be an undesired consequence, since both the white phosphorus and hypophosphorous acid methods of illicit methamphetamine production are significantly more hazardous methods. Given the small quantities and limited uses of these chemicals necessary for the production of methamphetamine, the DEA is proposing that no threshold be established for domestic and international transactions. Many of the transfers were for recovery or recycling and a few were for disposal in landfills. The study revealed that in those instances where the production method could be ascertained, red phosphorus was used in 87% of these laboratories. In case of eye contact Flush eyes with water as a precaution. It is considered to be the sodium salt of hypophosphorous acid. Chemical mixtures for these applications are formulated within a range of less than one percent to no greater than 20 percent in sodium hypophosphite. This notice proposes, therefore, that no threshold be established for domestic and international transactions. DEA List I status It is used as a water treatment agent and as a meat preservative. The Drug Enforcement Administration makes every effort to write clearly. Sodium Hypophosphite (DEA List I Chemical), FCC is used as an emulsifier and stabilizer. A black crystalline form of phosphorus is also occasionally made and is similar to graphite in its physical, thermal and electrical properties. Handlers of these chemicals will also be required to maintain records and meet CSA import/export notification requirements for "regulated transactions" of these chemicals. The analysis concluded that there are only two bulk manufacturers of phosphorus, most of whose product is sold to chemical manufacturers or exported. Interpretation Translation Examples of these salts include: Ammonium hypophosphite, calcium hypophosphite, iron hypophosphite, potassium hypophosphite, manganese hypophosphite, magnesium hypophosphite and sodium hypophosphite. The CSA, therefore, provides the Attorney General with authority to establish a threshold amount for "listed chemicals" if the Attorney General so elects. E-commerce Initiatives Source new and latest Sodium Hypophosphite products in 2020 from credible China manufacturers, suppliers and factories. Sodium hypophosphite monohydrate can be used as a: • Reducing agent in the synthesis of nickel nanoparticles (NiNP) from nickel acetate tetrahydrate under microwave irradiation. For phosphorus, compliance with EPA and DOT regulations should document distributions to customers and offsite waste transfers. The CSA (21 U.S.C. Chemical Control Program H 2 O. Elemental phosphorus is derived from phosphate rock. How Many Importers and Exporters Are Potentially Affected? It is used to prevent the discoloration of polymers. Deputy Administrator. Global Sodium Hypophosphite Market was valued US$ XX Mn in 2019 and is expected to reach US$ 975.12 Mn by 2026, at a CAGR of around XX % during a forecast period.. Additionally, a review of calendar years 1998-1999 clandestine laboratory seizure data (reported by the El Paso Intelligence Center and the Western States Information Network) indicated that more than 3750 seized methamphetamine laboratories were confirmed as utilizing phosphorus. Nonetheless, it is likely that chemical distributors do maintain records of shipments and customers even if shipping papers are not required. The lists are designated within The Controlled Substances Act, 21 U.S.C. The DEA is proposing that the white and red forms of elemental phosphorus be designated as List I chemicals. Additionally, two producers of hypophosphorous acid were identified. H2O. Registrant Record of Controlled Substances Destroyed Therefore, this action has not been reviewed by the Office of Management and Budget. Sodium hypophosphite (NaPO 2 H 2) is the sodium salt of hypophosphorous acid. Find here Sodium Hypophosphite manufacturers & OEM manufacturers India. Theft/Loss ReportingImport/Export This rule is not a major rule as defined by Section 804 of the Small Business Regulatory Enforcement Fairness Act of 1996. Rinse mouth with water. DEA has determined that this is not a significant rulemaking action. xH 2 O. Molecular Weight: 87.98 (anhydrous basis) CAS Number: 123333-67-5. ADDRESSES: Comments should be submitted in triplicate to the Deputy Administrator, Drug Enforcement Administration, Washington, DC 20537, Attention: DEA Federal Register Representative/CCR. DEA recognizes that these chemicals have legitimate industrial uses and that regulation of these phosphorus chemicals may have some effect upon certain industries. What Is Phosphorus Used for and How Large Is the Industry? In the form of white crystals, Sofibex is packaged in 25 kg bags, or in 500 and 1000 kg big bags. USA.GOV    |     Non-California customers must complete form QAF482. Therefore, this proposed regulation will only affect the distribution of less than 2% of the industry at the end user level. It is also used in the preparation of hypophosphite salts, which are in turn used in synthetic fibers as wetting agents, dispersing agents, anti-static agents and emulsifying agents. It is a solid at room temperature, appearing as odorless white crystals. It is soluble in … DEA's research indicates that there are currently only two domestic producers of elemental phosphorus. Sodium hypophosphite should be kept in a cool, dry place, isolated from … [2] The latter requires that the substrate is activated with fine particles of palladium. It is soluble in water, and easily absorbs moisture from the air. Physical. This proposed regulation is not considered to have an impact upon a substantial number of firms, given the limited distribution of these three chemicals. Availability. Questions & Answers JUSTICE.GOV    |     BILLING CODE 4410-09-P. NOTICE: This is an unofficial version. Sodium Hypophosphite (Monohydrate) CAS No 10039-56-2 MATERIAL SAFETY DATA SHEET SDS/MSDS . Batch: 100701/10547. Therefore the DEA believes that all transactions should be regulated, regardless of size, to prevent the diversion of these phosphorus chemicals to clandestine laboratories. Drug Disposal InformationDrug and Chemical Information Therefore, use of these alternate methods poses increased hazards for both law enforcement and for the public. Its assay is 810g/L, meaning a 60% solution. Diversion Control Division  •  8701 Morrissette Drive  •  Springfield, VA 22152  •  1-800-882-9539, DEA.GOV    |     The Idaho State Police, however, have closely monitored the illicit use of white phosphorus. California customers must complete form QAF481 and be advised that there is The Deputy Administrator hereby certifies that this rulemaking has been drafted in a manner consistent with the principles of the Regulatory Flexibility Act (5 U.S.C. DATA Waived Physicians It is soluble in water, and easily absorbs moisture from the air. Seized laboratories have historically identified seized material simply as 'phosphorus ' identified only two domestic producers of hypophosphorous acid indicates! Colorless hygroscopic solid, soluble in … Find here sodium hypophosphite Hydrate ( DEA List chemical. A Department of Justice Web site ( www.deadiversion.usdoj.gov ) only or white.! This poisonous gas can result in death is blended exclusively from high purity SHP for use in electroless nickel.. Allotropic ( i.e indicated that most all the material appeared to be affected by this regulation... 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